TOC-800
Process TOC Analyzer
The LFE TOC-800 has evolved out of real-world applications as an on-line analyzer for the continuous TOC registration of highly- as well as low contaminated water. The demands placed on every component of such an on-line TOC-analyzer require special design solutions. |
- Features
- Options
- VOC Analysis
- Technical Data
- Downloads
Features
- continuous analysis with high carbon conversion level (at up to 1100°C):
Only the high-temperature combustion method guarantees the nearly complete conversion of all organic carbon-compounds for the subsequent CO2-analysis. - extraordinarily stable measuring qualities:
High demands are placed on the stability of the system-components. For this reason, LFE developed a low-maintenance, high-precision metering pump for its on-line TOC-analyzers.
LFE's modified version of the BINOS® NDIR-photometer system is ideally suited because of it's excellent long-term stability and flexibility. - increased reliability:
Increased long term reliability is obtained through the enclosure of all electronic components, protecting them from adverse environments.
Separate cabinets for the analytical and the electronic components: The upper cabinet containing the NDIR-photometer as well as the majority of electrical components is purgable.
improved handling:
Maintenance and servicing of the instrument is facilitated through even better accessibility and handling.- outstanding reactor service-life:
The dimensioning of the analytical parameters allows maximum possible reactor service-life in combination with the fastest possible response time. - special detailed solutions:
The wetted components of the TOC-800 are composed of corrosion-resistant materials such as aluminum-oxide, glass and PTFE/PVDF.
The IR-photometer is fitted with an analysis cell specially developed by LFE. This cell is constructed out of glass with specially bonded sapphire windows. The extreme long-term stability of the NDIR-photometer is further enhanced by a patented gain controller. - intuitive User-Interface:
The TOC-800 is amazingly simple to operate despite its inherent complexity. The intuitive operation of the instrument is supported by a user-interface structure recommended by the NAMUR[1] commission. - automatic self-monitoring:
A wide range of system functions are continuously monitored. The intelligent self-monitoring places system failures into either of two categories: "maintenance required" or "instrument fault". The system status is available as floating relay-contacts and is displayed on the LC-display in plain text for easy diagnosis. - signal & status read-out:
The TOC-800 provides 4 individually-configurable, isolated 0(4)-20mA analog outputs. The available ranges (depending on instrument configuration) or even peripheral system values (e.g. reactor pressure) can be distributed over the 4 outputs.
In addition various status signals are available via the digital interface. The instrument status, among other things can be read out using the 3 floating contacts provided for this purpose. The contacts provide the following general information (according to NAMUR [1] recommendation): Instrument fault / Maintenance required / Maintenance
Options
- Acidifier/ Sparger/ Multiplexer-unit (ASM-unit; wall mounted)
The basic TOC-800 instrument functions as a TC-analyzer.
The ASM-unit facilitates the removal of inorganically bound carbon (TIC).
This unit can be equipped with further options:
- automatic calibration for 3 test solutions (1x zero level + 2x span solutions)
- Multiplex capability (3 sample streams)
- Dilution stage (max. dilution factor: 6) - simultaneous, selective VOC- or TIC- analysis
in conjunction with 2nd NDIR measuring channel and the Acidifier/ Sparger/ Multiplexer-unit - RS-232 serial interface
- built-in line recorder or data logger
VOC Analysis Package (optional)
Background
Aside from the intentional removal of inorganically bound carbon (TIC) the sparger air can also inadvertently expel volatile organic carbon (VOC) compounds which escape detection.
The TOC-800 can be fitted with an optional package in conjunction with a 2nd photometer channel which simultaneously and continuously measures the VOC-level independent of the TOC- (or DOC-) analysis.
Functional Principle
The potentially VOC enriched sparger air is split into two parallel gas streams each containing a CO2 background level representative of the TIC level of the water sample as well as possible VOC.
- The 1st gas stream is passed unaltered through the reference cell of the differential CO2 photometer channel.
- The 2nd gas stream is passed through a catalytic converter stage in which any VOC is oxidized to CO2 and added to the background CO2 level. This stream is sent to the sample side of the differential CO2 photometer.
The difference in IR radiation absorption in the photometer channel corresponds to the VOC concentration of the water sample.
The inherent response of a differential NDIR photometer to varying background levels is dynamically corrected for by the implementation of LFE's patented gain stabilization / common mode rejection algorithm. This is made possible by the use of a specially modified BINOS® photometer system (Emerson Process). First introduced by LFE in 1989, this unique method totally eliminates the need for a CO2 scrubber. The resultant maintenance requirements for the VOC analysis are minimal.
Technical Data
| Property | Specifications | |
| TOC-Analyzer (main instrument cabinet) | ||
| Cabinet | 2-section 19" cabinet on lockable rollers; active ventilation via filtered fans; electronics section purgeable |
|
| Dimensions (h x w x d) |
1680mm x 650mm x 650mm | |
| Acidifier / Sparger / Multiplexer unit (option) | ||
| Construction | Components on polypropylene panel for wall mounting | |
| available options | acidifier-/sparger stage, automatic calibration, stream multiplex, supplemental peristaltic bypass feed pumps | |
| Dimensions (h x w) | Basic unit: 500 x 500mm; Extended unit: 500 x 665mm | |
| Analytical-/Operational data | ||
| Measured quantity | Basic instrument: TC with optional sparger-unit: TOC/DOC as well as optional simultaneous VOC analysis |
|
TC/TOC/DOC |
VOC- measurement principle (optional) |
|
| Principle[2][3] | High temperature combustion (typically 950°C; adjustable up to 1100°C) of water sample with subsequent photometric CO2 analysis in the dried reactor exhaust (Peltier sample-gas cooler). Lowest range : 0 - 5 [mg C/l] Highest range : 0 - 5000 [mg C/l] |
Sparger air analyzed for volatile organic carbon components utilizing catalytic conversion with subsequent photometric CO2 analysis in a dedicated channel. The differential operation of this channel alleviates the need for a CO2-scrubber. Lowest range : 0 - 10 [mg VOC/l] Highest range : 0 - 300 [mg VOC/l] |
| Response Time[2] | t90: typically 5 min. (continuous analysis) |
t90: typically 2 min. (continuous analysis) |
| Precision[2] | better than ±1% of FSO | better than ±1% of FSO |
| Accuracy[2] | better than ±1% of FSO | better than ±2.5% of FSO |
| Inputs and outputs | ||
| Read-out | LC-display (40 characters x 16 lines) user interface based on NAMUR[1] recommendation |
|
| Analog signal output | 4 current outputs 0(4) - 20 mA (all outputs isolated and individually configurable) |
|
Digital inputs |
8 configurable inputs (6 – 24VDC; 10mA max.) Sample stream selection, calibration solution selection, AutoCal start/cancel |
|
| Digital outputs | 12 configurable outputs (relay contacts 28V max.; 350mA max.) Instrument status, sample stream feedback, calibration solution and AutoCal etc. |
|
| Instrument Status | Plain text description on the LC-display as well as categorization into one of the following states (NAMUR[1] recommendation): INSTRUMENT FAULT, MAINTENANCE REQUIRED, MAINTENANCE |
|
Downloads
The following documents are currently available for download in Adobe® PDF-format or in Microsoft® Word format:
| Product / Document type | Language | File name | File format | File size | |
| English | German | ||||
| TOC-800 - Online TOC-Analyzer | |||||
| Application questionnaire | | 21_appq_en.doc | | 165 KB | |
| Brochure | | 21_info_en.pdf | | 139 KB | |
| General information | |||||
| Brochure | | LFE_info_overview_en.pdf | | 118 KB | |
Technical specifications subject to change without notice
[1] NAMUR: Standardization commission for measuring and control technology in the chemical industry (sub-committee for operability of microprocessor-controlled process analytical- instrumentation)
[2] Data dependant on instrument configuration
[3] Range specifications using standard instrument parameters, without optional sample dilution.
Lower and higher ranges on request


The TOC-800 represents the newest generation of LFE's on-line TOC-analyzers. These have proven themselves with considerable success in use at many chemical plants as well as other important industrial companies since the beginning of the '80s.